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Have you paid attention to the details of rotary evaporator?

Article source:Have you paid attention to the details of rotary evaporator?  Hits:543  Release time:2021-01-15





The desktop rotary evaporator was developed by heidelf, Germany, which gathered hundreds of experts from all over the world to make suggestions and demands on the rotary evaporator during the use process, through actual contact with customers. In terms of design, experts constantly design and adjust through actual experience and demand, including evaporation tube jacket, anti reflux angle of condensation tube, surface area of 2200cm M2 condensation tube, LED ring indicator light, heating pot dumping handle... In terms of details, you have achieved the acme. In the actual use process, no matter from the safety or convenience of operation, you are all for rotary evaporation The overall use of Fayi has brought about a qualitative change, which truly reflects the concept of Heidolph's R & D team to assist scientific research.


For the rotary evaporator, good equipment is half of the success of the experiment. At the same time, how to operate the equipment correctly, improve the service life of the instrument and reduce the maintenance cost is also a topic of great concern to all scientific researchers.



 

用户案例一


 

用户案例二


In the process of using the rotary evaporator water bath pot, we often encounter the above two situations, no matter which one is not very beautiful, so how to solve it?


We know that most of the tanks of water bath pots are made of stainless steel. Stainless steel is the abbreviation of stainless acid resistant steel, which is resistant to air, steam, water and other weak corrosive media or stainless steel; while the steel resistant to chemical corrosive media (acid, alkali, salt and other chemical etching) is called acid resistant steel. Of course, there are grades of stainless steel materials. Different materials of stainless steel are used in different fields. Stainless steel has good thermal conductivity, and is durable and beautiful. At the same time, compared with other materials of water bath pot, stainless steel liner is more convenient in the removal of scale and other impurities. The main reason for the above two situations is that you heat the "water" used in the pot.





What kind of water do the experimenters put in the heating pot of the rotary evaporator during the experiment? Most experimenters choose deionized water. Unexpectedly, high purity deionized water is the culprit for the rust of water bath.


Deionized water (DI water) is a form of purified water that removes mineral ions such as sodium, calcium, iron, copper, chloride and bromide. Because the number of ions in deionized water can be controlled artificially, all deionized water is also widely used in the laboratory. So deionized water as a hot pot bath is feasible?



There are some acid-base problems in deionized water. When deionized water meets stainless steel, there will be some electrochemical reaction, that is charge transfer. As a result of this transfer, the electrons of metal elements in stainless steel will be absorbed and some anode electrons will be exposed. For example, when the positive valent iron ion encounters oxygen in the air, because the electrode potential of iron is always lower than that of oxygen, iron will be corroded as the negative electrode. We often see that there are many small bulges with different diameters after the heating pot has been used for a long time, that is, oxygen corrosion occurs on the surface of the heating pot, and the secondary layer is black powder ulcer corrosion pit, which leads to the damage of stainless steel containers. This is irreversible and we can't ignore it. This is one of the important reasons why high purity deionized water can not be stored or transported in stainless steel containers.


Similarly, distilled water or desalted water in the laboratory is not suitable for stainless steel heating pots. Distilled water usually refers to the water in which the anions and cations dissolved have been removed. Therefore, water tends to recover these cations and anions in order to saturate them again. So it became "hungry.". To satisfy hunger, water dissolves ions in the metal and carbon dioxide in the air, turning it into carbonic acid. This results in the pH value of distilled water around 5, that is, in the acidic range, the metal will be corroded.


Take good care of your heating pot, please do not use the above water quality for heating operation.









What kind of water should we use? Please use laboratory tap water. Tap water has low cost and is not easy to rust. It should be noted that in the use of tap water to operate the heating pot, for a period of time, scale accumulation will inevitably occur. Scale is the accumulation of calcium and magnesium in tap water. Due to the difference of hardness of water quality in different parts of the country, the hardness in the north is a little bit higher than that in the south, and the condition of the heating pot after using tap water is also slightly different. Although the scale has little effect on the heating pot itself, it has a great impact on the appearance, and it will also affect the heat conduction efficiency for a long time. Therefore, it is necessary to clean the scale regularly, which is also a necessary course for the maintenance of water bath in the laboratory.


To remove scale, we usually use baking soda, acetic acid, citric acid and so on. In the laboratory, Xiaohai recommends that you use low concentration citric acid to clean the water bath pot regularly. On the one hand, citric acid can effectively dissolve scale, making your water bath as new as ever. On the other hand, citric acid belongs to weak acid organic acid, does not contain chloride ion, and has the least damage to metal components, so it can protect the heating pot from damage.


In addition, we use tap water heating process, if you can add a certain proportion of pure water, can delay the formation of scale Oh!




Have you learned all these tips? If you still can't meet your requirements, please call 0512-67158275 to consult Suzhou hisiyuan. We provide you with the original heating bath and cleaning set provided by Heidolph, which will bring you a different experience.


Why don't you take care of your water bath? If you have any questions, please leave a message.





END


About Hei VAP heating pot

                              



characteristic


◇  The maximum temperature can reach 210 ℃

◇  A maximum of 5L evaporation bottle can be used

◇  It can move 200 mm horizontally

◇  In order to avoid short circuit and corrosion, the cable connection of heating pot meets IP67 protection standard

◇  The antiskid handle can avoid the risk of scald when dumping bath liquid

◇  The integral dumping port can safely dump bath liquid


About haisiyuan

                              


Suzhou hisiyuan instrument and Equipment Co., Ltd. is a professional service platform providing overall solutions for laboratories.


Mainly committed to providing customers with the whole process of basic laboratory services and a variety of basic equipment. It is widely used in hospitals, biomedicine, chemical industry, food, optoelectronics, testing, government departments and universities. Services include: laboratory design and decoration, consultation and guidance of various laboratory laws and regulations, laboratory maintenance and stable and reliable laboratory equipment.


The equipment includes cryogenic sample preservation system, liquid nitrogen storage system, pure water supply system, temperature and humidity monitor system, gel imaging system, centrifugal separation system, freeze drying system, biosafety and biological culture system, high temperature sterilization and cleaning system, high and low temperature control temperature verification system, etc.


Our professional service team is composed of technicians, sales personnel and maintenance personnel. We provide customers with all-round and one-stop service including technical consultation, product selection, door-to-door delivery, installation and debugging, operation training, maintenance, etc.


In line with the service concept of customer first, our company adheres to the enterprise values of integrity, fairness and perfection, so that customers can truly experience the butler service and relieve their worries.


Enterprise tenet: contribute to the cause of human health!


Enterprise vision: become a reliable enterprise! Grow into a respected enterprise!


Enterprise values: integrity, fairness and perfection!


Business philosophy: with timely and efficient service to solve problems for customers, with real sincere service customers! Result oriented, value for money!


Talent concept: understand a hard work, a harvest! Know how to be grateful!


For more details, please call 0512-67158275 or email HSY_ 007@hsy515.cn, we will serve you wholeheartedly.



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